• Home
  • Profil
    • Sejarah
    • Visi dan Misi
    • Organisasi
  • Program Studi
    • Sarjana Farmasi
    • Profesi Apoteker
    • Magister Farmasi
    • Magister Farmasi Klinik
    • Doktor Farmasi
    • International Class
    • Sertifikat Akreditasi Program Studi
  • Departemen
    • Analisis Farmasi dan Kimia Medisinal
    • Biologi Farmasi
    • Farmakologi dan Farmasi Klinik
    • Farmasetika dan Teknologi Farmasi
  • Informasi
    • Info Calon Mahasiswa
    • Fasilitas
    • Riset, Inovasi & Kerjasama
    • Berita
    • E Learning Fakultas
    • E Learning Unpad
  • Kemahasiswaan dan Alumni
    • Alumni
    • Kantor Internasional
      • Bahasa Indonesia
Fakultas Farmasi Universitas Padjadjaran
  • Home
  • Profil
    • Sejarah
    • Visi dan Misi
    • Organisasi
  • Program Studi
    • Sarjana Farmasi
    • Profesi Apoteker
    • Magister Farmasi
    • Magister Farmasi Klinik
    • Doktor Farmasi
    • International Class
    • Sertifikat Akreditasi Program Studi
  • Departemen
    • Analisis Farmasi dan Kimia Medisinal
    • Biologi Farmasi
    • Farmakologi dan Farmasi Klinik
    • Farmasetika dan Teknologi Farmasi
  • Informasi
    • Info Calon Mahasiswa
    • Fasilitas
    • Riset, Inovasi & Kerjasama
    • Berita
    • E Learning Fakultas
    • E Learning Unpad
  • Kemahasiswaan dan Alumni
    • Alumni
    • Kantor Internasional
      • Bahasa Indonesia

Berita

  • Home
  • Blog
  • Berita
  • The Development of Glucosamine Analysis in the Shark Cartilage Using High Performance Liquid ChromatographyThe Development of Glucosamine Analysis in the Shark Cartilage Using High Performance Liquid Chromatography

The Development of Glucosamine Analysis in the Shark Cartilage Using High Performance Liquid ChromatographyThe Development of Glucosamine Analysis in the Shark Cartilage Using High Performance Liquid Chromatography

  • Date 15 Maret 2012
  • Tags

Ida Musfiroh and Aliya Nur Hasanah

International Journal of Medical and Pharma Research (IJMPR).

 Vol. 1(1) : pp 9-15 (2011)

http://www.journalijmps.com/Dec2011.htm#R2

 The study is to analyze the development of glucosamine in the shark cartilage by employing High Performance Liquid Chromatography (HPLC) with UV-Vis detector. The analytical method is done by using the derivatization process considering the fact that glucosamine is a polar compound and has no sufficient chromophor to absorb UV radiation. The research is conducted through steps of shark cartilage mineral processing, that is, the preparation of standard and sample solution, the determination of optimum conditions, the validation of analytical methods, and the analysis of glucosamine in the shark cartilage respectively.
The validation of the analytical method is shown by these results: correlation coefficient of linearity test 0.995, variation coefficient of precision test 0.38% – 1.42%, recovery of accuration test 98.24 % – 101.95 %, resolution test (Rs) 1.975, LOD 0.24 ppm, and LOQ 0,80 ppm. The concentration of glucosamine in the shark cartilage is 1.08% at 240 nm UV detector, a C18 column (Lichocart (R), 250 mm x 4 mm), mobile phase aqua bidestilata: glassial acetic acid: methanol (89.96:0.04:10 pH 2.67) and a flow rate 1.2 ml / min.
Keywords:
Derivatization, HPLC, PITC, Reverse Phase, Shark Cartilage, UV Detector

 Ida Musfiroh, Aliya Nur Hasanah

http://www.journalijmps.com/Dec2011.htm#R2

International Journal of Medical and Pharma Research (IJMPR).

Vol. 1(1) : pp 9-15 (2011)

The study is to analyze the development of glucosamine in the shark cartilage by employing High Performance Liquid Chromatography (HPLC) with UV-Vis detector. The analytical method is done by using the derivatization process considering the fact that glucosamine is a polar compound and has no sufficient chromophor to absorb UV radiation. The research is conducted through steps of shark cartilage mineral processing, that is, the preparation of standard and sample solution, the determination of optimum conditions, the validation of analytical methods, and the analysis of glucosamine in the shark cartilage respectively.
The validation of the analytical method is shown by these results: correlation coefficient of linearity test 0.995, variation coefficient of precision test 0.38% – 1.42%, recovery of accuration test 98.24 % – 101.95 %, resolution test (Rs) 1.975, LOD 0.24 ppm, and LOQ 0,80 ppm. The concentration of glucosamine in the shark cartilage is 1.08% at 240 nm UV detector, a C18 column (Lichocart (R), 250 mm x 4 mm), mobile phase aqua bidestilata: glassial acetic acid: methanol (89.96:0.04:10 pH 2.67) and a flow rate 1.2 ml / min.
Keywords: Derivatization, HPLC, PITC, Reverse Phase, Shark Cartilage, UV Detector

  • Share:
author avatar
ffunpad

Previous post

Panduan Beasiswa Unggulan 2012Guidance for "Unggulan" Scholarship 2012
15 Maret 2012

Next post

Bahan kuliah farmasetika dasar 2012-AnggaPharmaceutic handout 2012-Angga
26 Maret 2012

You may also like

Top To Bottom: Gestures Basic Principles
5 Juni, 2022

Stats reveal that interaction is approximately 20% voice tonality, 20per cent real voiced language, and an astonishing 60per cent body gestures. Basically: it is not everything you point out that really matters – its just how you say it. Body …

On the web Visibility Tips for Men
23 Mei, 2022

There finding a mistressre plenty of posts authored for females looking to find Mr. Appropriate online, but not way too many are comprised with men in your mind. This indicates most relationship content articles are written for males by guys …

TDA international Radfahren: sicherer & aufregender Mittel für Daten den Planeten ganze Welt|die ganze Welt|Gesellschaft|weltweit|global} & Make Bleibende Kontakte
9 Mei, 2022

Der Brief Version: TDA Worldwide Radfahren ermutigt abenteuerlustige Singles und Paare treffen auf die offene Autobahn in atemberaubende Fernbedienung isoliert} Ziele auf sechs Kontinenten. Bedienen eines Fahrrads die in West Afrika oder im Stadtgebiet Straßen in Istanbul bietet Menschen unverwechselbare …

Leave A Reply Batalkan balasan

Alamat email Anda tidak akan dipublikasikan. Ruas yang wajib ditandai *

 

The faculty of excellence

Links

  • Konsorsium K-PPO
  • Jurnal IdJP
  • Jurnal IJCP
  • Jurnal PCPR
  • Jurnal IJPST
  • Jurnal Farmaka
  • Majalah Farmasetika
  • Info Calon Mahasiswa
  • E Learning Fakultas
  • PaUS ID
  • Portal Staffs
  • Repository
  • Perpustakaan
  • Layanan Terpadu
  • Foto Wisuda
  • farmasi@unpad.ac.id
  • www.farmasi.unpad.ac.id
  • Jl. Bandung-Sumedang KM 21
    Sumedang, 45363
  • 842 888888 Ext : 3510

Fakultas Farmasi, Universitas Padjadjaran. Copyright 2021